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Biomineralization-inspired copper-cystine nanoleaves capable of laccase-like catalysis for the colorimetricdetection of epinephrine

Miao Guan, Mengfan Wang, Wei Qi, Rongxin Su, Zhimin He

《化学科学与工程前沿（英文）》 2021年 第15卷 第2期   页码 310-318 doi: 10.1007/s11705-020-1940-y

摘要： Recently, many efforts have been dedicated to creating enzyme-mimicking catalysts to replace natural enzymes in practical fields. Inspired by the pathological biomineralization behaviour of L-cystine, in this study, we constructed a laccase-like catalyst through the co-assembly of L-cystine with Cu ions. Structural analysis revealed that the formed catalytic Cu-cystine nanoleaves (Cu-Cys NLs) possess a Cu(I)-Cu(II) electron transfer system similar to that in natural laccase. Reaction kinetic studies demonstrated that the catalyst follows the typical Michaelis-Menten model. Compared with natural laccase, the Cu-Cys NLs exhibit superior stability during long-term incubation under extreme pH, high-temperature or high-salt conditions. Remarkably, the Cu-Cys NLs could be easily recovered and still maintained 76% of their activity after 8 cycles. Finally, this laccase mimic was employed to develop a colorimetric method for epinephrine detection, which achieved a wider linear range (9–455 μmol·L ) and lower limit of detection (2.7 μmol·L ). The Cu-Cys NLs also displayed excellent specificity and sensitivity towards epinephrine in a test based on urine samples.

关键词： biomineralization     laccase     L-cystine     colorimetric detection     enzyme mimic    

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Label-free colorimetric nanosensor with improved sensitivity for Pb

Abdul Ghaffar Memon, Xiaohong Zhou, Yunpeng Xing, Ruoyu Wang, Lanhua Liu, Mohsin Khan, Miao He

《环境科学与工程前沿（英文）》 2019年 第13卷 第1期 doi: 10.1007/s11783-019-1094-7

摘要：

• Unmodified-AuNP based, colorimetric nanosensor was constructed for Pb2+ detection.

• 5-nucleotide truncation in DNAzyme made complete substrate detachment upon Pb2+.

• Ultrasensitive and selective detection of Lead (II) was achieved with 0.2×10-9 mol/L LOD.

关键词： Colorimetric nanosensor     Truncated 8–17 DNAzyme     Pb2+ detection     Unmodified AuNPs    

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A simple, azulene-based colorimetric probe for the detection of nitrite in water

Lloyd C. Murfin, Carlos M. López-Alled, Adam C. Sedgwick, Jannis Wenk, Tony D. James, Simon E. Lewis

《化学科学与工程前沿（英文）》 2020年 第14卷 第1期   页码 90-96 doi: 10.1007/s11705-019-1790-7

摘要： We describe the synthesis and evaluation of an azulene-based chemodosimeter for nitrite. The probe was found to undergo two distinct color changes upon introduction aqueous nitrite ion. A near-instant formation of a grey color provides a qualitative indication of the presence of nitrite, followed by the formation of a deep-yellow/orange color, the endpoint from which quantitative data can be derived. The azulene probe exhibits 1:1 stoichiometry of reaction with nitrite in water, and is selective for nitrite over other anions. The azulene probe was applied to determine nitrite content in cured meat, and compared with the British Standard testing procedure (Griess test). The value obtained from the azulene-based probe agreed closely with the standard test. Our procedure only requires the preparation of one standard solution, instead of the three required for the standard Griess test.

关键词： azulene     nitrite     diazoquinone    

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A cellphone-based colorimetric multi-channel sensor for water environmental monitoring

《环境科学与工程前沿（英文）》 2022年 第16卷 第12期 doi: 10.1007/s11783-022-1590-z

摘要：

● A cellphone-based colorimetric multi-channel sensor for in-field detection.

关键词： Colorimetric analysis     Multi-channel sensor     Cellphone     Water quality indexes     Environmental monitoring    

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A novel flavonol-based colorimetric and turn-on fluorescent probe for rapid determination of hydrazine

《化学科学与工程前沿（英文）》 2023年 第17卷 第1期   页码 24-33 doi: 10.1007/s11705-022-2171-1

摘要： Hydrazine is extremely toxic and causes severe harm to human body. Herein, a novel fluorescent probe 4-oxo-2-styryl-4H-chromen-3-yl thiophene-2-carboxylate (FHT) was synthesized for detecting hydrazine by using natural cinnamaldehyde as starting material. This probe exhibited significantly enhanced fluorescence response towards hydrazine over various common metal ions, anions, and amine compounds. The detection limit of probe FHT for hydrazine was as low as 0.14 μmol·L–1, significantly lower than that of the threshold value of 0.312 μmol·L–1, imposed by the Environmental Protection Agency. Moreover, the proposed probe was able to detect hydrazine within wide pH (5–10) and linear detection ranges (0–110 μmol·L–1). This probe was employed for determining trace hydrazine in different environmental water samples. The probe FHT-loaded filter paper strips were able to conveniently detect hydrazine of low concentration through distinct naked-eye and fluorescent color changes. Importantly, the probe FHT with low cytotoxicity was successfully applied to visualize hydrazine in living Hela cells and zebrafish.

关键词： cinnamaldehyde     3-hydroxychromone derivative     hydrazine     fluorescent probe    

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A review of measurement methods for peracetic acid (PAA)

Chen Cheng, Haodong Li, Jinling Wang, Hualin Wang, Xuejing Yang

《环境科学与工程前沿（英文）》 2020年 第14卷 第5期 doi: 10.1007/s11783-020-1266-5

摘要： Abstract • Physical and chemical properties and application of peracetic acid solution. • Determination method of high concentration peracetic acid. • Determination method of residual peracetic acid (low concentration). Peroxyacetic acid has been widely used in food, medical, and synthetic chemical fields for the past several decades. Recently, peroxyacetic acid has gradually become an effective alternative disinfectant in wastewater disinfection and has strong redox capacity for removing micro-pollutants from drinking water. However, commercial peroxyacetic acid solutions are primarily multi-component mixtures of peroxyacetic acid, acetic acid, hydrogen peroxide, and water. During the process of water treatment, peroxyacetic acid and hydrogen peroxide (H2O2) often coexist, which limits further investigation on the properties of peroxyacetic acid. Therefore, analytical methods need to achieve a certain level of selectivity, particularly when peroxyacetic acid and hydrogen peroxide coexist. This review summarizes the measurement and detection methods of peroxyacetic acid, comparing the principle, adaptability, and relative merits of these methods.

关键词： Peroxyacetic acid     Measurement methods     Titration     Colorimetric     Chromatography     NMR    

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Usability perceptions and beliefs about smart thermostats by chi-square test, signal detection theory, and fuzzy detection theory in regions of Mexico

Pedro PONCE, Therese PEFFER, Arturo MOLINA

《能源前沿（英文）》 2019年 第13卷 第3期   页码 522-538 doi: 10.1007/s11708-018-0562-2

摘要： It is well known that smart thermostats (STs) have become key devices in the implementation of smart homes; thus, they are considered as primary elements for the control of electrical energy consumption in households. Moreover, energy consumption is drastically affected when the end users select unsuitable STs or when they do not use the STs correctly. Furthermore, in future, Mexico will face serious electrical energy challenges that can be considerably resolved if the end users operate the STs in a correct manner. Hence, it is important to carry out an in-depth study and analysis on thermostats, by focusing on social aspects that influence the technological use and performance of the thermostats. This paper proposes the use of a signal detection theory (SDT), fuzzy detection theory (FDT), and chi-square (CS) test in order to understand the perceptions and beliefs of end users about the use of STs in Mexico. This paper extensively shows the perceptions and beliefs about the selected thermostats in Mexico. Besides, it presents an in-depth discussion on the cognitive perceptions and beliefs of end users. Moreover, it shows why the expectations of the end users about STs are not met. It also promotes the technological and social development of STs such that they are relatively more accepted in complex electrical grids such as smart grids.

关键词： thermostats     perceptions     beliefs     signal detection theory (SDT)     fuzzy signal detection theory (FSDT)     chi-square (CS) test    

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Advances in airborne microorganisms detection using biosensors: A critical review

《环境科学与工程前沿（英文）》 2021年 第15卷 第3期 doi: 10.1007/s11783-021-1420-8

摘要：

Humanity has been facing the threat of a variety of infectious diseases. Airborne microorganisms can cause airborne infectious diseases, which spread rapidly and extensively, causing huge losses to human society on a global scale. In recent years, the detection technology for airborne microorganisms has developed rapidly; it can be roughly divided into biochemical, immune, and molecular technologies.

关键词： Biosensor     Airborne microorganisms     Microbiological detection technology    

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Recent advances in SERS detection of perchlorate

Jumin Hao, Xiaoguang Meng

《化学科学与工程前沿（英文）》 2017年 第11卷 第3期   页码 448-464 doi: 10.1007/s11705-017-1611-9

摘要： Perchlorate has recently emerged as a widespread environmental contaminant of healthy concern. Development of novel detection methods for perchlorate with the potential for field use has been an urgent need. The investigation has shown that surface-enhanced Raman scattering (SERS) technique has great potential to become a practical analysis tool for the rapid screening and routine monitoring of perchlorate in the field, particularly when coupled with portable/handheld Raman spectrometers. In this review article, we summarize progress made in SERS analysis of perchlorate in water and other media with an emphasis on the development of SERS substrates for perchlorate detection. The potential of this technique for fast screening and field testing of perchlorate-contaminated environmental samples is discussed. The challenges and possible solutions are also addressed, aiming to provide a better understanding on the development directions in the research field.

关键词： perchlorate     SERS     detection     substrate     modification     nanostructure    

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A fast antibiotic detection method for simplified pretreatment through spectra-based machine learning

《环境科学与工程前沿（英文）》 2022年 第16卷 第3期 doi: 10.1007/s11783-021-1472-9

摘要：

• A spectral machine learning approach is proposed for predicting mixed antibiotic.

关键词： Antibiotic contamination     Spectral detection     Machine learning    

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Anthocyanins/chitosan films doped by nano zinc oxide for active and intelligent packaging: comparison of anthocyanins source from purple tomato or black wolfberry

《化学科学与工程前沿（英文）》 2023年 第17卷 第6期   页码 704-715 doi: 10.1007/s11705-022-2270-z

摘要： The multifunctional films was prepared by blending chitosan and nano-ZnO with purple tomato anthocyanins or black wolfberry anthocyanins. The properties of films functioned by anthocyanins source and nano-ZnO content were studied. It was found purple tomato anthocyanins showed more significant color change against pH than black wolfberry anthocyanins. The nano-ZnO were widely dispersed in matrix and enhanced the compatibility of anthocyanins with chitosan. However, the anthocyanins source influenced the properties of the films more slightly than nano-ZnO addition. The tensile strength, antioxidant and antibacterial effects of the chitosan films dramatically increased after cooperated by nano-ZnO and anthocyanins, which also enhanced with increase of nano-ZnO content, whereas the elongation at break of the composite films decreased. Especially, the anthocyanin and nano-ZnO promoted the antibacterial activity of films synergistically. Composite films made from black wolfberry anthocyanins exhibited higher mechanical performance than those made from purple tomato anthocyanins but weaker antibacterial effects. The purple tomato anthocyanins/chitosan and nano-ZnO/purple tomato anthocyanins/chitosan films effectively reflected pork spoilage, changing their colors from dark green to brown, indicating the potential for applications in active and intelligent food packaging.

关键词： bio-based     multifunction     colorimetric indicator     active and intelligent packaging    

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脉冲辐射探测技术

欧阳晓平

《中国工程科学》 2008年 第10卷 第4期   页码 44-55

摘要：

脉冲辐射探测是探知核反应过程特征信息的主要途径之一，是核反应过程特性研究、核装置设计、运行、监测与控制不可或缺的技术手段。由核探测器、探测方法和应用技术等构成的脉冲辐射场探测技术，已成为科学研究、核技术应用、核材料分析、裂变/聚变研究和天体物理等相关核科学研究的必备技术元素。文章介绍了我国发展的瞬态核裂变、核聚变反应过程释放的脉冲中子、伽马混合辐射场探测系统和测量技术。

关键词： 裂变反应     聚变反应     脉冲辐射探测     探测系统     中子测量     伽马测量    

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Edge detection of steel plates at high temperature using image measurement

Qiong Zhou, Qi An

《机械工程前沿（英文）》 2009年 第4卷 第1期   页码 77-82 doi: 10.1007/s11465-009-0013-1

摘要： An edge detection method for the measurement of steel plate’s thermal expansion is proposed in this paper, where the shrinkage of a steel plate is measured when temperature drops. First, images are picked up by an imaging system; a method of regional edge detection based on grayscales’ sudden change is then applied to detect the edges of the steel plate; finally, pixel coordinates of the edge position are transformed to physical coordinates through calibration parameters. The experiment shows that the real-time, high precision, and non-contact measurement of the steel plate’s edge position under high temperature can be realized using the imaging measurement method established in this paper.

关键词： thermal expansion     image measurement     edge detection     image calibration    

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Machine vision-based automatic fruit quality detection and grading

《农业科学与工程前沿（英文）》 doi: 10.15302/J-FASE-2023532

摘要：

● A machine vision-based prototype system was developed for fruit grading.

关键词： Computer and machine vision     convolution neural network     deep learning     defective fruit detection     fruit grading     microcontroller    

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Experimental and numerical study on microcrack detection using contact nonlinear acoustics

Xiaojia CHEN, Yuanlin WANG

《结构与土木工程前沿（英文）》 2009年 第3卷 第2期   页码 137-141 doi: 10.1007/s11709-009-0028-z

摘要： This paper introduces a non-classical nonlinear acoustic theory for microcrack detection in materials, comparing contact nonlinearity with material nonlinearity. The paper’s main work concentrates on the experimental and numerical verification of the effectivity of contact nonlinear acoustic detection by using the contact nonlinear parameter , which can be represented by the ratio of the second-harmonic amplitude to the square of the first-harmonic amplitude. Both experiments and numerical tests are performed. The results show that is sensitive to the initiation of microcracks and varies with the development of the microcracks. The numerical test illustrates the decline of when microcracks penetrate each other.

关键词： microcrack detection     contact nonlinearity     numerical analysis    

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标题 作者 时间 类型 操作

Biomineralization-inspired copper-cystine nanoleaves capable of laccase-like catalysis for the colorimetricdetection of epinephrine

Miao Guan, Mengfan Wang, Wei Qi, Rongxin Su, Zhimin He

期刊论文

Label-free colorimetric nanosensor with improved sensitivity for Pb

Abdul Ghaffar Memon, Xiaohong Zhou, Yunpeng Xing, Ruoyu Wang, Lanhua Liu, Mohsin Khan, Miao He

期刊论文

A simple, azulene-based colorimetric probe for the detection of nitrite in water

Lloyd C. Murfin, Carlos M. López-Alled, Adam C. Sedgwick, Jannis Wenk, Tony D. James, Simon E. Lewis

期刊论文

A cellphone-based colorimetric multi-channel sensor for water environmental monitoring

期刊论文

A novel flavonol-based colorimetric and turn-on fluorescent probe for rapid determination of hydrazine

期刊论文

A review of measurement methods for peracetic acid (PAA)

Chen Cheng, Haodong Li, Jinling Wang, Hualin Wang, Xuejing Yang

期刊论文

Usability perceptions and beliefs about smart thermostats by chi-square test, signal detection theory, and fuzzy detection theory in regions of Mexico

Pedro PONCE, Therese PEFFER, Arturo MOLINA

期刊论文

Advances in airborne microorganisms detection using biosensors: A critical review

期刊论文

Recent advances in SERS detection of perchlorate

Jumin Hao, Xiaoguang Meng

期刊论文

A fast antibiotic detection method for simplified pretreatment through spectra-based machine learning

期刊论文

Anthocyanins/chitosan films doped by nano zinc oxide for active and intelligent packaging: comparison of anthocyanins source from purple tomato or black wolfberry

期刊论文

脉冲辐射探测技术

欧阳晓平

期刊论文

Edge detection of steel plates at high temperature using image measurement

Qiong Zhou, Qi An

期刊论文

Machine vision-based automatic fruit quality detection and grading

期刊论文

Experimental and numerical study on microcrack detection using contact nonlinear acoustics

Xiaojia CHEN, Yuanlin WANG

期刊论文